Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the. ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Copper – Copper Sulfate – 16% sulfuric acid, ASTM A – Practice E (Strauss Test). ASTM A Practice E test. This practice describes the procedure by which the copper-copper sulfate% sulfuric acid test is conducted to determine .
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ASTM A Intergranular Corrosion Testing and Analysis
Sample condition before soaking in Ferric chloride solution. Test sample was etched using Oxalic Acid with electrolyte etching. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
Intergranular corrosion shows up as the dark black lines around the grain boundaries. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. It depends on which Practice is selected, but typically ranges from to days for different tests. Examination of intergranular cracks and fissures on bend surface. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals.
It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.
Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours.
The corrosion test has the advantage of being relatively rapid, requiring 24 hours plus sample preparation time. Intergranular cracking or crazing is evidence of astmm. Although this test method uses some similar equipment, this method should not be confused with Test Method G Link to Active This link will always route to the current Active version of the standard.
This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.
A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization. Corrosion Tests are conducted to determine the resistance of a metal to chemical attack.
This method is a hour boiling test for “as received” specimens of stainless steel. This abstract is a brief summary of the referenced standard. Please share this page: ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. The level of corrosion is determined by mass loss. For example, many low-carbon and stabilized stainless steels e.
Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.
Due to the variance of attack in different materials, numerous methods Pracfice B-F are used to assess intergranular corrosion. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on. Bend Specimen after soaking. The test uses a visual inspection of the surface of the bent specimen to determine pass or fail.
This test method does not determine the critical pitting temperature or test for the suitability for use in a particular environment. Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasesprachice as sigma phase, that occurs along the grain boundaries. All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. Corrosion test is measured by weight loss per area of test sample.
Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. This test is used exclusively to determine corrosion in areas high in chromium pracice formations, and is not as effective for intergranular attack caused by other means.
The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades.
If you are not sure, practife contact us for assistance. Work Item s – proposed revisions of this standard. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date. These test d determine the relative pitting resistance of stainless steel and nickel-base, chromium bearing alloys. In everyday applications, corrosion varies by materials and solutions. Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.
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